Author(s):
Mieaad Mohammed, Nagham Mahmood Aljamali, Wassan Ala Shubber, Sabreen Ali Abdalrahman
Email(s):
Dr.Nagham_mj@yahoo.com
DOI:
10.5958/0974-360X.2018.00472.9 
Address:
Mieaad Mohammed1, Dr. Nagham Mahmood Aljamali2, Wassan Ala Shubber2, Sabreen Ali Abdalrahman2
1Assistant Lecturer, Chemistry Department, Faculty of Sciences, Iraq.
2Department of Chemistry, Faculty of Education, Iraq.
*Corresponding Author
Published In:
Volume - 11,
Issue - 6,
Year - 2018
ABSTRACT:
Cyclization reaction has been used to preparation of series heterocyclic azo- azomethine ligands through many steps, the first step: esterification of carboxylic terminal, then cyclization of ester with thiosemicarbazide, followed by second step which involved azotation of amino group of thiadiazole, the third step was reacted with di carbonyl compound, the last step involved cyclization with compounds containing di nucleophile groups to yield series azo heterocyclic – azomethine ligands. The resulting ligands were investigated bymany techniques like (1H NMR, FT.IR andUV-Visible spectra) with biological test.
Cite this article:
Mieaad Mohammed, Nagham Mahmood Aljamali, Wassan Ala Shubber, Sabreen Ali Abdalrahman. New Azomethine- Azo Heterocyclic Ligands Via Cyclization of Ester. Research J. Pharm. and Tech 2018; 11(6): 2555-2560. doi: 10.5958/0974-360X.2018.00472.9
Cite(Electronic):
Mieaad Mohammed, Nagham Mahmood Aljamali, Wassan Ala Shubber, Sabreen Ali Abdalrahman. New Azomethine- Azo Heterocyclic Ligands Via Cyclization of Ester. Research J. Pharm. and Tech 2018; 11(6): 2555-2560. doi: 10.5958/0974-360X.2018.00472.9 Available on: https://www.rjptonline.org/AbstractView.aspx?PID=2018-11-6-73